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CHEMISTRY

Interpretations and Questions Concerning this Synthesis
Interpretation of IR (Infrared Spectrometry)
By running an infrared spectrometry (IR) important information about
the particular functional groups of a compound is obtained. This allows
for the naming of an unknown compound by analyzing the different
functional groups that makes up the specific compound. The regions in
which the functional groups appear fall between 4000-1300 cm-1 on the
spectra. Since the compound I attempted to synthesize was an ester, the
first thing I looked for on my spectra was a strong peak between
1800-1700 cm-1. My spectra did indeed have a strong peak at 1718.6 cm-1
so I concluded that the functional group ester was present in my
compound. The, part of the compound is represented by a peak at cm-1 on
the spectra that I ran. The that is located on the end of my compound
shows up in the spectra by the peaks that occur between cm-1. After
analyzing the spectra that I ran on my compound, I compared the IR
results to the one in Sadtler. Since they were the same, I was able to
confirm that the compound I synthesized was indeed isopentyl acetate.
Interpretation of NMR (Nuclear Magnetic Resonance Spectrometry)
The significance or running a nuclear magnetic resonance spectrometry
(NMR)
Is that this test gives useful information that leads to the ability to
determine where the H+ are located in the compound. In isopentyl
acetate there are 4 different arrangements of the H+ that add up to all
10 H+ which make up the compound. The three H+ located on the ester part
of the molecule is seen in my NMR by the single peak between 3.7-4.1
ppm. This peak is single because it isn¡¯t involved in any spin-spin
interactions that cause splitting. The two separate H+ that are involved
in the are recognizable in my spectra as the two single peaks seen
between ppm.
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